4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: synthesis and comparative structural and spectroscopic analyses

Kumru, Ufuk; DUMOULIN , FABIENNE; Jeanneau, Erwann; Yuksel, Fatma; Cabezas, Yari; Zorlu, Yunus; Ahsen, Vefa

doi:10.1007/s11224-011-9850-8

4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: synthesis and comparative structural and spectroscopic analyses

Kumru U., DUMOULIN F., Jeanneau E., Yuksel F., Cabezas Y., Zorlu Y., ...Daha Fazla

STRUCTURAL CHEMISTRY, cilt.23, sa.1, ss.175-183, 2012 (SCI-Expanded, Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 23 Sayı: 1
Basım Tarihi: 2012
Doi Numarası: 10.1007/s11224-011-9850-8
Dergi Adı: STRUCTURAL CHEMISTRY
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.175-183
Anahtar Kelimeler: Phthalonitrile, tert-Butanethiol, tert-Butylsulfanylphthalonitrile, Single-crystal, IR, NMR, Structural analysis, NON-PERIPHERAL POSITIONS, SUBSTITUTED PHTHALOCYANINES, NUCLEOPHILIC-SUBSTITUTION, EMERGING APPLICATIONS, ELECTRONIC-PROPERTIES, PHTHALONITRILES, TETRACHLOROPHTHALONITRILE, ANALOGS, DYES
Acıbadem Mehmet Ali Aydınlar Üniversitesi Adresli: Hayır

Özet

Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.