4,5-, 3,6-, and 3,4,5,6-tert-Butylsulfanylphthalonitriles: synthesis and comparative structural and spectroscopic analyses


Kumru U., DUMOULIN F. , Jeanneau E., Yuksel F., Cabezas Y., Zorlu Y., ...More

STRUCTURAL CHEMISTRY, vol.23, no.1, pp.175-183, 2012 (Journal Indexed in SCI) identifier identifier

  • Publication Type: Article / Article
  • Volume: 23 Issue: 1
  • Publication Date: 2012
  • Doi Number: 10.1007/s11224-011-9850-8
  • Title of Journal : STRUCTURAL CHEMISTRY
  • Page Numbers: pp.175-183

Abstract

Three tert-butylsulfanylphthalonitriles have been prepared with optimized synthetic procedures. Their comparative structural analyses have been completed, with a focus on IR and NMR spectroscopy and refined X-ray structural data. Miscellaneous parameters such as UV absorption, melting points, and related polarity of the compounds are summarized.